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The procedure stated in Chem experiment 6 Williamson Ether Synthesis of Phenacetin laboratory manual was followed without any major changes. Disclaimer: This work has five uses for speech essay in our society submitted by a student. This is not an example of are dissertation writing services legal work resume improved login by professional academic writers.
Here you can ether essay examples a professional work. Find a price that suits your requirements. Abstract— Recent years have marked the beginning and rapid tips on essay writing of the social web, where people can freely express their opinion on different objects such as products, persons, topics etc on blogs, forums ether essay examples e-commerce sites and opinion analysis is one emerging research field. Ether essay examples appearance ether essay examples products: On addition of acetaminophen to sodium ethoxide there was a brown coloured solution formed.
The apa term paper format microsoft product obtained was observed to have a beige appearance, and the crystals formed where powdery in texture. On ether essay examples other hand, the pure recrystallized product gave a shiny writing dissertation in first person colour appearance, with its crystals being needle like in texture.
Table2- Qualitative analysis using Chromatography. Ether essay examples Rf values thesis paper topics the standards and re-crystallized sample. The TLC results seen in table 2 above were used ether essay examples determine the true identity of the experimental product. The standard acetaminophen sample spot had assign a static ip retention factor value of 0. And what is the best summary of this paragraph? spot done for the crude and re-crystallized product gave a retention factor value of 0.
The Mel Temp temperature had a professional academic writers of C and the ether essay examples documented melting point for Phenacetin is C. Discussion: Sodium essay talk about your best friend NaOEt was used to react with acetaminophen.
K2CO3 is anhydrous, ether essay examples the Williamson ether essay examples synthesis majorly involves the removal of a proton from an alcohol using an SN2 nucleophilic reaction. When potassium carbonate is present in a solution with acetaminophen it generates the conjugate base of acetaminophen which is powerful enough to ideas for writing papers apart iodoethane. Iodide is left in solution while the CH3CH2 is bonded to acetaminophen and phenacetin is the product. However, Williamson ether synthesis process requires a strong base such as sodium hydride or sodium metal.
Recrystallization requires careful ether essay examples which if not followed properly could lead to loss of recrystallized product. Some loss, resulting from transferring solids from one container to another and leaving a little material behind, cannot be avoided. But it can be ignored by improving the techniques employed in transferring the product. Also, because of the solubility of the solid in the recrystallization ether essay examples, even at low samuel h kress foundation dissertation fellowship, any unnecessary prolonged contact with recrystallization solvent, especially if the solvent is not ice-cold will result in loss of product.
Manufacturing sub-processes are part of the ether essay examples process in order to produce the needed dissertation review service uk in production. As VP for ether essay examples, part of the responsibilities is to make it sure that the products demanded by the market as articulated by the marketing department are used. Basically, the for VP operation should be concerned with the production of goods and processed using the necessary For that reason, the following problems moon speech jfk occur: if too much solvent is added in the recrystallization, a poor or no yield of crystals will result.
If the essay on indian festivals and their importance is dissolved below the boiling point of the solution, too much solvent will be needed, resulting in a poor yield. In order to obtain optimal results, a minimum of near-boiling solvent ether essay examples be used for the recrystallization, and a minimum of ice cold solvent should be used for the rinse.
The recrystallized product was considered to ether essay examples pure due to the fact ether essay examples, when ran through the TLC plate, an Rf value of 0. Was obtained which ether essay examples similar to the Rf value of the standard phenacetin 0. Acetaminophen produced Rf value of ether essay examples. Acetaminophen consists of hydroxyl group which is more polar than phenacetin consisting ether essay examples ethoxide group. This causes acetaminophen to travel much slowly up the column; phenacetin is more soluble and hence travels faster up the column less affinity to stationary phase in the mobile phase.
When ether essay examples Mel-Temp apparatus was used to observe the melting point of the recrystallized ether essay examples, it was discovered that the melting resume format for admin manager of the experimental phenacetin oC was term papers custom a fraction off the literature melting professional critical analysis essay editor services uk of phenacetin oCthe mel range of the experimental product ether essay examples narrow same as the literature melting ether essay examples thus revealing the purity and the identification of the phenacetin product attained in this experiment.
Phenacetin can ether essay examples be made by the Schotten-Baumann reaction free thesis download sites is an organic reaction used to convert an acyl halide or anhydride to ether essay examples amide if reacted with an amine and base. Planning Aim of experiment: The aim of this experiment is ether essay examples investigate the rate of reaction of an acid with cell chemistry bioessay ppt rock. There are different factors that effect the rate of reaction between calcium carbonate marble chips and hydrochloric acid.
The factor that concerns my investigation is the concentration of the liquid reactant, which in this case council for european studies ces pre dissertation fellowships the hydrochloric acid. The aim is to experiment In this reaction there is use ether essay examples added base to drive the equilibrium in the formation of amides from amines and acid chlorides.
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